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Summary
Summary
With over 17,000 articles concerning NMR published per year, keeping up to date with the latest developments and applications of this technique can prove time-consuming. Now in its 42nd volume, the Specialist Periodical Report on NMR provides a digest of the current literature, compiled by experts in the field.
The current volume devotes several chapters to the aspects and applications of spin-spin couplings, and biochemists will find seperate chapters dedicated to proteins, lipids and carbohydrates. Further chapters discuss the latest developments in nuclear sheilding, imaging and NMR in living systems.
For a comprehensive account of the latest developments and research using NMR, look no further than Specialist Periodical Reports - Nuclear Magnetic Resonance. An essential book for NMR lab and university shelf.
Author Notes
Professor Krystyna Kamienska-Trela is based at the Institute of Organic Chemistry, Polish Academy of Sciences, Warsaw.
Table of Contents
Preface | p. v |
Books and reviews | p. 1 |
Books | p. 1 |
Regular reviews series | p. 1 |
Edited books and symposia | p. 6 |
Reviews in periodicals | p. 21 |
Reviews and books in foreign languages | p. 37 |
Theoretical and physical aspects of nuclear shielding | p. 45 |
1 Theoretical aspects of nuclear shielding | p. 45 |
2 Physical aspects of nuclear shielding | p. 58 |
References | p. 70 |
Applications of nuclear shielding | p. 78 |
1 Introduction | p. 78 |
2 Shielding of particular nuclear species | p. 78 |
References | p. 131 |
Theoretical aspects of indirect spin-spin couplings | p. 152 |
1 Introduction | p. 152 |
2 Application of calculated indirect spin-spin couplings to the compounds exhibiting conformational or rotational flexibility | p. 154 |
3 Application of calculated indirect spin-spin couplings to investigation of compounds with pnicogen bonds and complexes between electron/proton donors and acceptors | p. 160 |
4 Compounds with hydrogen bonds | p. 163 |
5 Through space indirect spin-spin couplings | p. 165 |
6 New methods and benchmark calculations | p. 167 |
7 Calculation of indirect spin-spin couplings including relativistic effects | p. 169 |
8 Various works | p. 170 |
9 Indexes | p. 173 |
References | p. 174 |
Applications of spin-spin couplings | p. 181 |
1 Introduction | p. 181 |
2 New methods | p. 183 |
3 Scalar nuclear spin-spin coupling in van der Waals molecules | p. 185 |
4 One-bond couplings to hydrogen | p. 186 |
5 One-bond couplings not involving hydrogen | p. 189 |
6 Two-bond couplings to hydrogen | p. 195 |
7 Two-bond couplings not involving hydrogen | p. 198 |
8 Three-bond hydrogen-hydrogen couplings | p. 199 |
9 Three-bond couplings to hydrogen | p. 206 |
10 Three-bond couplings not involving hydrogen | p. 208 |
11 Couplings over more than three bonds and through space | p. 209 |
12 Couplings through hydrogen bonds | p. 211 |
13 Residual dipolar couplings | p. 213 |
14 The splittings in the NMR spectra under near-zero-field nuclear (NZF) conditions | p. 216 |
References | p. 217 |
Nuclear spin relaxation in liquids and gases | p. 230 |
1 Introduction | p. 939 |
2 General, physical and experimental aspects of nuclear spin-relaxation | p. 231 |
3 Selected applications of nuclear spin relaxation in liquids | p. 247 |
4 Nuclear spin relaxation in gases | p. 263 |
Acknowledgements | p. 264 |
References | p. 264 |
Solid state NMR spectroscopy | p. 276 |
1 Introduction | p. 276 |
2 Reviews | p. 276 |
3 Experimental and computational developments | p. 282 |
4 Applications | p. 295 |
References | p. 322 |
NMR of proteins and nucleic acids | p. 331 |
1 Introduction | p. 331 |
2 New methodology | p. 332 |
3 High-resolution structural studies | p. 343 |
4 NMR studies of large biomolecules | p. 350 |
References | p. 355 |
NMR of lipids | p. 362 |
1 Introduction | p. 362 |
2 The structures and cellular functions of lipids | p. 363 |
3 Interactions of lipids with proteins, peptides and small molecules | p. 366 |
4 Lipids in biomedicine | p. 371 |
5 NMR-based methodology | p. 374 |
Abbreviations used | p. 374 |
Acknowledgments | p. 375 |
References | p. 375 |
NMR of carbohydrates | p. 383 |
1 Introduction | p. 383 |
2 Determination of sugar structure | p. 383 |
3 Non-covalent interactions | p. 396 |
4 Identification and quantification of sugars | p. 400 |
5 New NMR methods for sugar analysis | p. 401 |
6 Computational NMR methods and sugar databases | p. 401 |
References | p. 402 |
Synthetic macromolecules | p. 420 |
1 Introduction | p. 420 |
2 Primary structure | p. 420 |
3 Imaging and diffusion | p. 429 |
4 Characterization of the synthetic macromolecules | p. 430 |
5 Dynamics and polymer blend of the synthetic macromolecules | p. 432 |
References | p. 434 |
NMR of liquid crystals and micellar solutions | p. 450 |
1 Introduction | p. 450 |
2 General articles: reviews, methods, models | p. 452 |
3 Liquid crystals | p. 453 |
4 Micellar solutions | p. 474 |
References | p. 491 |
NMR in living systems | p. 498 |
1 New methods, hardware and localisation | p. 498 |
2 Pre-clinical studies | p. 500 |
3 Clinical studies | p. 504 |
References | p. 521 |
Oriented molecules | p. 535 |
1 Introduction | p. 535 |
2 Reviews, theory and general studies | p. 536 |
3 New techniques and novel orienting media | p. 538 |
4 Studies of oriented small molecules including chiral systems | p. 541 |
5 Novel mesophases and orientational order | p. 546 |
6 Relaxation and dynamic NMR studies | p. 550 |
7 Membranes and molecules oriented therein | p. 553 |
8 Weak ordering and biomolecular studies | p. 557 |
References | p. 563 |