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Cover image for Nuclear magnetic resonance
Title:
Nuclear magnetic resonance
Series:
Specialist periodical reports ; 42
Publication Information:
Cambridge : Royal Society of Chemistry, 2013
Physical Description:
xix, 572 p. ; 24 cm.
ISBN:
9781849735773

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30000010319060 QC762 N833 2013 Open Access Book Book
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Summary

Summary

With over 17,000 articles concerning NMR published per year, keeping up to date with the latest developments and applications of this technique can prove time-consuming. Now in its 42nd volume, the Specialist Periodical Report on NMR provides a digest of the current literature, compiled by experts in the field.

The current volume devotes several chapters to the aspects and applications of spin-spin couplings, and biochemists will find seperate chapters dedicated to proteins, lipids and carbohydrates. Further chapters discuss the latest developments in nuclear sheilding, imaging and NMR in living systems.

For a comprehensive account of the latest developments and research using NMR, look no further than Specialist Periodical Reports - Nuclear Magnetic Resonance. An essential book for NMR lab and university shelf.


Author Notes

Professor Krystyna Kamienska-Trela is based at the Institute of Organic Chemistry, Polish Academy of Sciences, Warsaw.


Table of Contents

Krystyna Kamienska-TrelaWojciech SchilfCynthia J. Jameson and Angel C. De DiosShigeki Kuroki and Tsunenori Kameda and Hidekazu YasunagaJaroslaw JazwinskiKrystyna Kamienska-Trela and Jacek WójcikJozef KowalewskiA. E. Aliev and R. V. LawPeter J. SimpsonSlawomir Pikula and Joanna Bandorowicz-Pikula and Patrick GrovesDaniel Lowicki and Agnieszka Czarny and Jacek MlynarskiHiromichi Kurosu and Takeshi YamanobeGerardino D 'Errico and Luigi PaduanoM. J. W. PriorY. Jayasubba Reddy and K. V. Ramanathan
Prefacep. v
Books and reviewsp. 1
Booksp. 1
Regular reviews seriesp. 1
Edited books and symposiap. 6
Reviews in periodicalsp. 21
Reviews and books in foreign languagesp. 37
Theoretical and physical aspects of nuclear shieldingp. 45
1 Theoretical aspects of nuclear shieldingp. 45
2 Physical aspects of nuclear shieldingp. 58
Referencesp. 70
Applications of nuclear shieldingp. 78
1 Introductionp. 78
2 Shielding of particular nuclear speciesp. 78
Referencesp. 131
Theoretical aspects of indirect spin-spin couplingsp. 152
1 Introductionp. 152
2 Application of calculated indirect spin-spin couplings to the compounds exhibiting conformational or rotational flexibilityp. 154
3 Application of calculated indirect spin-spin couplings to investigation of compounds with pnicogen bonds and complexes between electron/proton donors and acceptorsp. 160
4 Compounds with hydrogen bondsp. 163
5 Through space indirect spin-spin couplingsp. 165
6 New methods and benchmark calculationsp. 167
7 Calculation of indirect spin-spin couplings including relativistic effectsp. 169
8 Various worksp. 170
9 Indexesp. 173
Referencesp. 174
Applications of spin-spin couplingsp. 181
1 Introductionp. 181
2 New methodsp. 183
3 Scalar nuclear spin-spin coupling in van der Waals moleculesp. 185
4 One-bond couplings to hydrogenp. 186
5 One-bond couplings not involving hydrogenp. 189
6 Two-bond couplings to hydrogenp. 195
7 Two-bond couplings not involving hydrogenp. 198
8 Three-bond hydrogen-hydrogen couplingsp. 199
9 Three-bond couplings to hydrogenp. 206
10 Three-bond couplings not involving hydrogenp. 208
11 Couplings over more than three bonds and through spacep. 209
12 Couplings through hydrogen bondsp. 211
13 Residual dipolar couplingsp. 213
14 The splittings in the NMR spectra under near-zero-field nuclear (NZF) conditionsp. 216
Referencesp. 217
Nuclear spin relaxation in liquids and gasesp. 230
1 Introductionp. 939
2 General, physical and experimental aspects of nuclear spin-relaxationp. 231
3 Selected applications of nuclear spin relaxation in liquidsp. 247
4 Nuclear spin relaxation in gasesp. 263
Acknowledgementsp. 264
Referencesp. 264
Solid state NMR spectroscopyp. 276
1 Introductionp. 276
2 Reviewsp. 276
3 Experimental and computational developmentsp. 282
4 Applicationsp. 295
Referencesp. 322
NMR of proteins and nucleic acidsp. 331
1 Introductionp. 331
2 New methodologyp. 332
3 High-resolution structural studiesp. 343
4 NMR studies of large biomoleculesp. 350
Referencesp. 355
NMR of lipidsp. 362
1 Introductionp. 362
2 The structures and cellular functions of lipidsp. 363
3 Interactions of lipids with proteins, peptides and small moleculesp. 366
4 Lipids in biomedicinep. 371
5 NMR-based methodologyp. 374
Abbreviations usedp. 374
Acknowledgmentsp. 375
Referencesp. 375
NMR of carbohydratesp. 383
1 Introductionp. 383
2 Determination of sugar structurep. 383
3 Non-covalent interactionsp. 396
4 Identification and quantification of sugarsp. 400
5 New NMR methods for sugar analysisp. 401
6 Computational NMR methods and sugar databasesp. 401
Referencesp. 402
Synthetic macromoleculesp. 420
1 Introductionp. 420
2 Primary structurep. 420
3 Imaging and diffusionp. 429
4 Characterization of the synthetic macromoleculesp. 430
5 Dynamics and polymer blend of the synthetic macromoleculesp. 432
Referencesp. 434
NMR of liquid crystals and micellar solutionsp. 450
1 Introductionp. 450
2 General articles: reviews, methods, modelsp. 452
3 Liquid crystalsp. 453
4 Micellar solutionsp. 474
Referencesp. 491
NMR in living systemsp. 498
1 New methods, hardware and localisationp. 498
2 Pre-clinical studiesp. 500
3 Clinical studiesp. 504
Referencesp. 521
Oriented moleculesp. 535
1 Introductionp. 535
2 Reviews, theory and general studiesp. 536
3 New techniques and novel orienting mediap. 538
4 Studies of oriented small molecules including chiral systemsp. 541
5 Novel mesophases and orientational orderp. 546
6 Relaxation and dynamic NMR studiesp. 550
7 Membranes and molecules oriented thereinp. 553
8 Weak ordering and biomolecular studiesp. 557
Referencesp. 563
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