Cover image for Practical instrumental analysis : methods, quality assurance and laboratory management
Title:
Practical instrumental analysis : methods, quality assurance and laboratory management
Personal Author:
Publication Information:
Weinheim : Wiley-VCH, 2013
Physical Description:
xxiii, 467 p. : ill. ; 24 cm.
ISBN:
9783527329519

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30000010315205 QD79.I5 P48 2013 Open Access Book Book
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Summary

Summary

This practical book in instrumental analytics conveys an overview of important methods of analysis and enables the reader to realistically learn the (principally technology-independent) working techniques the analytical chemist uses to develop methods and conduct validation. What is to be conveyed to the student is the fact that analysts in their capacity as problem-solvers perform services for certain groups of customers, i.e., the solution to the problem should in any case be processed in such a way as to be "fit for purpose".
The book presents sixteen experiments in analytical chemistry laboratory courses. They consist of the classical curriculum used at universities and universities of applied sciences with chromatographic procedures, atom spectrometric methods, sensors and special methods (e.g. field flow fractionation, flow injection analysis and N-determination according to Kjeldahl).
The carefully chosen combination of theoretical description of the methods of analysis and the detailed instructions given are what characterizes this book. The instructions to the experiments are so detailed that the measurements can, for the most part, be taken without the help of additional literature.
The book is complemented with tips for effective literature and database research on the topics of organization and the practical workflow of experiments in analytical laboratory, on the topic of the use of laboratory logs as well as on writing technical reports and grading them (Evaluation Guidelines for Laboratory Experiments).
A small introduction to Quality Management, a brief glance at the history of analytical chemistry as well as a detailed appendix on the topic of safety in analytical laboratories and a short introduction to the new system of grading and marking chemicals using the "Globally Harmonized System of Classification and Labelling of Chemicals (GHS)", round off this book.
This book is therefore an indispensable workbook for students, internship assistants and lecturers (in the area of chemistry, biotechnology, food technology and environmental technology) in the basic training program of analytics at universities and universities of applied sciences.


Author Notes

After his apprenticeship, Sergio Petrozzi worked as a chemical lab technician at the Laboratory of Physical Chemistry ETHZ (Swiss Federal Institute of Technology) and at the Swiss Federal Institute of Aquatic Sciences and Technology (EAWAG), Switzerland. After acquiring his federal diploma (Diplom Hohere Fachprufung), he joined the Institute of Chemical Engineering ETHZ where he gained great experience as teaching assistant in laboratory courses. His daily routine focused among other topics, on the following topics at the ETHZ in Zurich: Development, optimization and validation of analytical methods. He subsequently worked as an application chemist at Buchi Labortechnik AG, Flawil (Switzerland) with a focus on the validation of applications for environmental determinations. He has authored numerous publications in international journals and is presently employed as a Scientific Associate at the Zurich University of Applied Sciences ZHAW, Wadenswil (Switzerland), where, among other things, he is teaching adviser in analytical chemistry laboratory at the Institute for Chemistry and Biological Chemistry (ICBC).


Table of Contents

Introduction
An Introduction To Quality Management
Basic Statistics
The Analytical Process
Validation Strategy
Planning An Experiment
Organizational And Practical Aspects
Literature
Projects
Chromatography
HPLC
GC
IC
LC-MS
GC-MS
Spectroscopy
UV-VIS
FTIR
NIR
AAS
NMR
X-Ray Fluorescence
Electrochemical Analysis
Coulometry
The Karl Fischer Method
Automation
Flow Injection Analysis
Other Analytical Methods
The Kjeldahl Method for N/Protein Analysis
Determination of Dissolved Oxygen
Appendix. Recommended Further Reading
Appendix. Statistic Tables
Appendix. Commitment
Appendix. Evaluation Guidelines
Appendix. Analytical Laboratory Safety