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Summary
Summary
How to use nuclear magnetic resonance imaging in chemical engineering.
Written by the internationally recognized top experts from academia and industry, this first book dedicated to the topic provides an overview of existing methods and strategies to solve individual problems in chemical engineering. Written in a simple and lively manner and backed by various industrial examples, the book begins with a look at hardware and methods, continuing on to cover porous materials, fluids and flow of increasing complexity from different fields of Chemical Engineering, before finishing off with a review of reactors and reactions.
The result allows engineers, industrial and academic researchers and decision-makers to gain a detailed insight into the NMR toolbox, such that they can estimate the benefit of NMR imaging with regard to cost efficiency and scientific results.
Author Notes
Siegfried Stapf received his PhD in Physics at the University of Ulm, Germany, in 1996. Following a postdoctoral stay at the University of Nottingham, UK, he currently holds a position as Hochschuldozent at the RWTH Aachen, Germany. His main research interests cover the fields of molecular dynamics and order of confined fluids and soft matter, as well as transport phenomena and structure/dynamics relations in complex media investigated with advanced Nuclear Magnetic Resonance Imaging techniques.
Song-I Han received her Doctoral Degree in Natural Sciences (Dr.rer.nat) from Aachen University of Technology, Germany, in 2001. She was awarded with the first Raymond Andrew Prize of the Ampere Society for an outstanding PhD thesis in magnetic resonance imaging. She pursued her postdoctoral studies at the University of California, Berkeley under the sponsorship of the Feodor Lynen Fellowship of the Alexander von Humboldt Foundation. Dr. Han joined as an Assistant Professor the Department of Chemistry and Biochemistry at the University of California, Santa Barbara in 2004. Her research expertise lies in magnetic resonance flow imaging methodologies and her research objectives are technique developments for orders of magnitude faster and more sensitive NMR spectroscopy and imaging.
Table of Contents
| 1 IntroductionSiegfried Stapf and Song-I. Han |
| 1.1 A Brief Comment |
| 1.2 The Very Basics of NMR |
| 1.3 Fundamentals of NMR Imaging |
| 1.4 Fundamentals of Detecting Motion |
| 1.5 Bringing Them Together: Velocity Imaging |
| 1.6 More Advanced Techniques I: Multiple Encoding and Multiple Dimensions |
| 1.7 More Advanced Techniques II: Fast Imaging Techniques |
| 1.8 Introducing Color into the Image: Contrast Parameters |
| 2 Hardware and Methods |
| 2.1 Hardware, Software and Areas of Application of Non-medical MRID. Gross and K. Zick and T. Oerther and V. Lehmann and A. Pampel and J. Goetz |
| 2.2 Compact MRI for Chemical EngineeringKatsumi Kose |
| 2.3 Drying of Coatings and Other Applications with GARFieldP. J. Doughty and P. J. McDonald |
| 2.4 Depth Profiling by Single-sided NMRF. Casanova and J. Perlo and B. Blumich) |
| 2.5 Microcoil NMR for Reaction MonitoringLuisa Ciobanu and Jonathan V. Sweedler and Andrew G. Webb |
| 2.6 Broadening the Application Range of NMR and MRI by Remote DetectionSong-I Han and Josef Granwehr and Christian Hilty |
| 2.7 Novel Two Dimensional NMR of Diffusion and Relaxation for Material CharacterizationYi-Qiao Song |
| 2.8 Hardware and Method Development for NMR RheologyPaul T. Callaghan |
| 2.9 Hydrodynamic, Electrodynamic and Thermodynamic Transport in Porous Model Objects: Magnetic Resonance Mapping Experiments and SimulationsElke Kossel and Bogdan Buhai and Rainer Kimmich |
| 3 Porous Materials |
| 3.1 Diffusion in Nanoporous MaterialsJorg Karger and Frank Stallmach and Rustem Valiullin and Sergey Vasenkov |
| 3.2 Application of Magnetic Resonance Imaging to the Study of the Filtration ProcessR. Reimert and E. H. Hardy and A. von Garnier |
| 3.3 Multiscale Approach to Catalyst DesignXiaohong Ren and Siegfried Stapf and Bernhard Blumich |
| 3.4 Pure Phase Encode Magnetic Resonance Imaging of Concrete Building MaterialsJ. J. Young and T. W. Bremner and M. D. A. Thomas and B. J. Balcom |
| 3.5 NMR Imaging of Functionalized CeramicsS. D. Beyea and D. O. Kuethe and A. McDowell and A. Caprihan and S. J. Glass |
| 3.6 NMR Applications in Petroleum Reservoir StudiesGeorge J. Hirasaki |
| 3.7 NMR Pore Size Measurements Using an Internal Magnetic Field in Porous MediaYi-Qiao Song and Eric E. Sigmund and Natalia V. Lisitza |
| 4 Fluids and Flows |
| 4.1 Modeling Fluid Flow in Permeable MediaJinsoo Uh and A. Ted Watson |
| 4.2 MRI ViscometerRobert L. Powell |
| 4.3 Imaging Complex Fluids in Complex GeometriesY. Xia and P. T. Callaghan |
| 4.4 Quantitative Visualization of Taylor-Couette-Poiseuille Flows with MRI+John G. Georgiadis and L.Guy Raguin and Kevin W. Moser |
| 4.5 Two Phase Flow of EmulsionsNina C. Shapley and Marcos A. d'Avila |
| 4.6 Fluid Flow and Trans-membrane Exchange in a Hemodialyzer ModuleSong-I Han and Siegfried Stapf |
| 4.7 NMR for Food Quality ControlMichael J. McCarthy and Prem N. Gambhir and Artem G. Goloshevsky |
| 4.8 Granular Flow (Eiichi Fukushima) |
| 5 Reactors and Reactions |
| 5.1 Magnetic Resonance Microscopy of Biofilm and Bioreactor TransportSarah L. Codd and Joseph D. Seymour and Erica L. Gjersing and Justin P. Gage and Jennifer R. Brown |
| 5.2 Two-phase Flow in Trickle-Bed ReactorsLynn F. Gladden and Laura D. Anadon and Matthew H.M. Lim and Andrew J. Sederman |
| 5.3 Hyperpolarized 129Xe NMR Spectroscopy, MRI and Dynamic NMR Microscopy for the In Situ Monitoring of Gas Dynamics in Opaque Media Including Combustion ProcessesGalina E. Pavlovskaya and Thomas Meersmann |
| 5.4 In Situ Monitoring of Multiphase Catalytic Reactions at Elevated Temperatures by MRI and NMRIgor V. Koptyug and Anna A. Lysova |
| 5.5 In Situ Reaction Imaging in Fixed-bed Reactors Using MRILynn F. Gladden and Belinda S. Akpa and Michael D. Mantle and Andrew J. Sederman |
