Available:*
Library | Item Barcode | Call Number | Material Type | Item Category 1 | Status |
---|---|---|---|---|---|
Searching... | 30000010321240 | TP159.D5 L89 2013 | Open Access Book | Book | Searching... |
On Order
Summary
Summary
Learn how to develop optimal steady-state designs for distillation systems
As the search for new energy sources grows ever more urgent, distillation remains at the forefront among separation methods in the chemical, petroleum, and energy industries. Most importantly, as renewable sources of energy and chemical feedstocks continue to be developed, distillation design and control will become ever more important in our ability to ensure global sustainability.
Using the commercial simulators Aspen Plus® and Aspen Dynamics®, this text enables readers to develop optimal steady-state designs for distillation systems. Moreover, readers will discover how to develop effective control structures. While traditional distillation texts focus on the steady-state economic aspects of distillation design, this text also addresses such issues as dynamic performance in the face of disturbances.
Distillation Design and Control Using Aspen (tm) Simulation introduces the current status and future implications of this vital technology from the perspectives of steady-state design and dynamics. The book begins with a discussion of vapor-liquid phase equilibrium and then explains the core methods and approaches for analyzing distillation columns. Next, the author covers such topics as:
Setting up a steady-state simulation Distillation economic optimization Steady-state calculations for control structure selection Control of petroleum fractionators Design and control of divided-wall columns Pressure-compensated temperature control in distillation columnsSynthesizing four decades of research breakthroughs and practical applications in this dynamic field, Distillation Design and Control Using Aspen (tm) Simulation is a trusted reference that enables both students and experienced engineers to solve a broad range of challenging distillation problems.
Author Notes
WILLIAM L. LUYBEN, PhD, is Professor of Chemical Engineering at Lehigh University where he has taught for over forty-five years. Dr. Luyben spent nine years as an engineer with Exxon and DuPont. He has published fourteen books and more than 250 original research papers. Dr. Luyben is a 2003 recipient of the Computing Practice Award from the CAST Division of the AIChE. He was elected to the Process Control Hall of Fame in 2005. In 2011, the Separations Division of the AIChE recognized his contributions to distillation technology by a special honors session.
Table of Contents
Preface |
Chapter 1 Fundamentals of VLE |
1.1 Vapor pressure |
1.2 Binary VLE phase diagrams |
1.3 Physical property methods |
1.4 Relative volatility |
1.5 Bubblepoint calculations |
1.6 Ternary diagrams |
1.7 VLE non-ideality |
1.8 Residue curves for ternary systems |
1.9 Distillation Boundaries |
1.10 Conclusion |
Chapter 2 Analysis of Distillation Columns |
2.1 Design degrees of freedom |
2.2 Binary McCabe-Thiele method |
2.3 Approximate multi-component methods |
2.4 Conceptual design of ternary systems |
2.5 Conclusion |
Chapter 3 Setting Up a Steady-State Simulation |
3.1 Configuring a new simulation |
3.2 Specifying chemical components and physical properties |
3.3 Specifying stream properties |
3.4 Specifying parameters of equipment |
3.5 Running the simulation |
3.6 Using design spec/vary function |
3.7 Finding the optimum feed tray and minimum conditions |
3.8 Column sizing |
3.9 Using Conceptual Design |
3.10 Conclusion |
Chapter 4 Distillation Economic Optimization |
4.1 Heuristic optimization |
4.2 Economic basis |
4.3 Results |
4.4 Operating optimization |
4.5 Optimum pressure for vacuum columns |
4.6 Conclusion |
Chapter 5 More Complex Distillation Systems |
5.1 Extractive distillation |
5.2 Heterogeneous azeotropic distillation |
5.3 Pressure-swing azeotropic distillation |
5.4 Heat-integrated columns |
5.5 Conclusion |
Chapter 6 Steady-State Calculations for Control Structure Selection |
6.1 Control structure alternatives |
6.2 Feed-composition sensitivity analysis |
6.3 Temperature control tray selection |
6.4 Conclusion |
Chapter 7 Converting from Steady State to Dynamic Simulation |
7.1 Equipment sizing |
7.2 Exporting to Aspen Dynamics |
7.3 Opening the dynamic simulation in Aspen Dynamics |
7.4 Installing basic controllers |
7.5 Installing temperature and composition controllers |
7.6 Performance evaluation |
7.7 Conclusion |
Chapter 8 Control of More Complex Columns |
8.1 Extractive distillation process |
8.2 Columns with partial condensers |
8.3 Control of heat-integrated distillation columns |
8.4 Control of azeotropic columns/decanter system |
8.5 Unusual Control Structure |
8.6 Conclusion |
Chapter 9 Reactive Distillation |
9.1 Introduction |
9.2 Types of reactive distillation systems |
9.3 TAME process basics |
9.4 TAME reaction kinetics and VLE |
9.5 Plantwide control structure |
9.6 Conclusion |
Chapter 10 Control of Sidestream Columns |
10.1 Liquid sidestream column |
10.2 Vapor sidestream column |
10.3 Liquid sidestream column with stripper |
10.4 Vapor sidestream column with rectifier |
10.5 Sidestream purge column |
10.6 Conclusion |
Chapter 11 Control of Petroleum Fractionators |
11.1 Petroleum fractions |
11.2 Characterization of crude oil |
11.3 Steady-state design of preflash column |
11.4 Control of preflash column |
11.5 Steady-state design of pipestill |
11.6 Control of pipestill |
11.7 Conclusion |
Chapter 12 Design and Control of Divided-Wall Columns |
12.1 Introduction |
12.2 Steady-state design |
12.3 Control of divided-wall columns |
12.4 Control of conventional column process |
12.5 Conclusion and Discussion |
Chapter 13 Dynamic Safety Analysis |
13.1 - Introduction |
13.2 - Safety scenarios |
13.3 - Process studied |
13.4 - Basic Radfrac models |
13.5 Dynamic simulations |
13.6 Comparison of dynamic responses |
13.7 Other Issues |
13.8 Conclusion |
Chapter 14 Carbon Dioxide Capture |
14.1 - Carbon dioxide removal in low-pressure air combustion power plants |
14.2 - Carbon dioxide removal in high-pressure IGCC power plants |
14.3 - Conclusion |
Chapter 15 Distillation Turndown |
15.1 Introduction |
15.2 Control problem |
15.3 Process studied |
15.4 Dynamic Performance for ramp disturbances |
15.5 Dynamic performance for step disturbances |
15.6 Other control structures |
15.7 Conclusion |
Chapter 16 Pressure-Compensated Temperature Control in Distillation Columns |
16.1 Introduction |
16.2 Numerical example studied |
16.3 Conventional control structure selection |
16.4 Temperature/pressure/composition relationships |
16.5 Implementation in Aspen Dynamics |
16.6 Comparison of dynamic results |
16.7 Conclusion |