Cover image for Electron crystallography : electron microscopy and electron diffraction
Title:
Electron crystallography : electron microscopy and electron diffraction
Personal Author:
Publication Information:
Oxford, ENK. ; New York : Oxford University Press, 2011.
Physical Description:
viii, 331 p. : ill. ; 26 cm.
ISBN:
9780199580200
General Note:
Includes bibliographical references and index

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30000010296601 QD906.7.E37 Z68 2011 Open Access Book Book
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Summary

Summary

In the modern world of ever smaller devices and nanotechnology, electron crystallography emerges as the most important method capable of determining the structure of minute objects down to the size of individual atoms. Crystals of only a few millionths of a millimetre are studied. This is the first textbook explaining how this is done. Great attention is given to symmetry in crystals and how it manifests itself in electron microscopy and electron diffraction, and how this symmetry can be determined and taken advantage of in achieving improved electron microscopy images and solving crystal structures from electron diffraction patterns.Theory and practice are combined; experimental images, diffraction patterns, formulae and numerical data are discussed in parallel, giving the reader a complete understanding of what goes on inside the "black boxes" of computer programs.This up-to-date textbook contains the newest techniques in electron crystallography, including detailed descriptions and explanations of the recent remarkable successes in determining the very complex structures of zeolites and intermetallics. The controversial issue of whether there is phase information present in electron micrsocopy images or not is also resolved once and for all. The extensive appendices include computer labs which have been used at various courses at Stockholm University and international schools in electron crystallography, with applications to the textbook. Students can download image processing programs and follow these lab instructions to get a hands-on experience of electron crystallography.


Author Notes

Xiaodong Zou and Sven Hovmller are professors of structural chemistry and Peter Oleynikov is a researcher, all at Stockholm University.


Table of Contents

1 Electron crystallography - an introductionp. l
2 Fundamental crystallographyp. 17
3 Crystal structure factors and symmetryp. 42
4 Fundamental transmission electron microscopyp. 72
5 Electron diffraction (ED)p. 90
6 Phase contrast, contrast transfer function (CTF) and high-resolution electron microscopy (HRTEM)p. 131
7 Solving crystal structures from HRTEM images by crystallographic image processingp. 156
8 Experimental procedures of crystallographic image processingp. 177
9 Solving crystal structures from ED datap. 191
10 Structure refinementp. 213
11 3D electron crystallographyp. 223
12 Simulation of images and electron diffraction patternsp. 245
13 Applications of electron crystallographyp. 254
Appendicesp. 268
Indexp. 321